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In reading about Synthesis of Essential Drugs, I have found in my lab (not a very good book, from a chemical point of view, a lot of mistakes), I have come upon a very strange way to synthesize benzodiazepines (actually triazolobenzodiazepines).

This synthesis starts by a nucleophilic substitution of hydrazine on a 2-chloroquinoline (2,6-dichloro-4-phenylquinoline), boiling this hydrazinoquinoline with orthoacetate in xylene affords triazoloquinoline intermediates.

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How you can access, change or suppress your Personal Information: If you would like to review, correct, update, suppress or delete Personal Information that you have previously provided to us, you may contact us at [email protected], or: Marriott International, Inc.and its affiliates, including The Ritz-Carlton Hotel Company, L. C., values you as our guest and recognizes that privacy is important to you.We want you to be familiar with how we collect, use and disclose information.Please note that we may need to retain certain information for recordkeeping purposes and/or to complete any transactions that you began prior to requesting a change or deletion (e.g., when you make a purchase or reservation, or enter a promotion, you may not be able to change or delete the Personal Information provided until after the completion of such purchase, reservation, or promotion).There may also be residual information that will remain within our databases and other records, which will not be removed.This intermediate undergoes the key step of the synthesis, a oxidative ring opening of the quinoline with sodium periodate and ruthenium oxide, leading to the triazolobenzophenone.

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